The sample had been subjected to heat prior to the testing procedure, and it still remains an unknown material.
If wood or coconut shell, that would have been revealed under examination by microscopy.
Don't you agree ?
The following extracts provide the background and detail to that:
First of all, only a small part of the sample was heated as a way of extracting and measuring the nitrogen content.
5.6.19 The sample was logged into the ORAU system in the usual manner
and, as in all cases, a sample of bone powder was drilled from the
underside of the specimen using a tungsten carbide drill. The powder
weighed 440 mg. The technician performing this procedure noted that
the material did not behave as bone ordinarily would and did not have
the texture that normal bone exhibits. The technician has a great deal
of experience in the sampling of bone (almost 30 years). Because of
this uncertainty, and as a precaution,
a small amount of the sample
was combusted to measure the % nitrogen remaining. % N is a good
correlate for protein, which is dominated in bone by collagen, and the
measurement of nitrogen offers a simple test concerning whether the
sample is dateable or not. Low % N means that the material is
essentially un-dateable using radiocarbon.
The analysis process seems to have been pretty comprehensive and came to the conclusion that is was wood.
5.6.4 Three days later, Forensic Services Manager X was contacted by X , also from the Oxford laboratory, confirming this uncertainty. X stated that X believed Exhibit JAR/6 to be coconut or wood ‘On 31st March' 08, I spoke to X in the laboratory and then made an examination of the exhibit immediately. I immediately recognised that the sample was NOT bone and stated that to X . I based my conclusions on the lightness of the material, the texture of the material and the porosity of the internal structure of the sample. I then consulted with a colleague, X of the British Museum, taking the sample with me for X to see. In X opinion, X, after examination,
agreed with my conclusions that the sample was not bone, but another material, that is, wood. I made the
decision to consult with X and contact X to inform X as to my findings, that same day. I telephoned X that same day’. The sample was then returned to store at Haut de la Garenne on 4 April 2008.
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You mentioned microscopy - I really cannot see how use of a scanning electron microscope would have helped as the difference between bone and wood is obvious at a cellular level, (optical micropscope) and does not need to be considered at a molecular level (Scanning electon microscope).